bcTol: a highly water-soluble biradical for efficient dynamic nuclear polarization of biomolecules
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Dagsetning
Höfundar
Journal Title
Journal ISSN
Volume Title
Útgefandi
Royal Society of Chemistry (RSC)
Úrdráttur
Dynamic nuclear polarization (DNP) is an efficient method to overcome the inherent low sensitivity of magic-angle spinning (MAS) solid-state NMR. We report a new polarizing agent (bcTol), designed for biological applications, that yielded an enhancement value of 244 in a microcrystalline SH3 domain sample at 110 K.
Lýsing
Post-print (lokagerð höfundar)
Efnisorð
Angle spinning NMR, Solid state, Nitroxide biradicals, Magnetic resonance, Amyloid fibrils, Protein, Resolution, Spectroscopy, Agents, Litrófsgreining, Segulmagn, Prótín, Kjarnsýrur
Citation
Jagtap, A. P., Geiger, M. -A., Stöppler, D., Orwick-Rydmark, M., Oschkinat, H., & Sigurdsson, S. T. (2016). BcTol: A highly water-soluble biradical for efficient dynamic nuclear polarization of biomolecules. Chemical Communications, 52(43), 7020-7023. doi:10.1039/c6cc01813k