Háskóli ÍslandsUniversity of IcelandJagtap, Anil P.Geiger, Michel-AndreasStöppler, DanielOrwick-Rydmark, MarcellaOschkinat, HartmutSigurdsson, Snorri2020-08-102020-08-102016Jagtap, A. P., Geiger, M. -A., Stöppler, D., Orwick-Rydmark, M., Oschkinat, H., & Sigurdsson, S. T. (2016). BcTol: A highly water-soluble biradical for efficient dynamic nuclear polarization of biomolecules. Chemical Communications, 52(43), 7020-7023. doi:10.1039/c6cc01813k1359-73451364-548X (eISSN)https://hdl.handle.net/20.500.11815/1959Post-print (lokagerð höfundar)Dynamic nuclear polarization (DNP) is an efficient method to overcome the inherent low sensitivity of magic-angle spinning (MAS) solid-state NMR. We report a new polarizing agent (bcTol), designed for biological applications, that yielded an enhancement value of 244 in a microcrystalline SH3 domain sample at 110 K.7020-7023eninfo:eu-repo/semantics/openAccessAngle spinning NMRSolid stateNitroxide biradicalsMagnetic resonanceAmyloid fibrilsProteinResolutionSpectroscopyAgentsLitrófsgreiningSegulmagnPrótínKjarnsýrurinfo:eu-repo/semantics/articleChemical Communications10.1039/C6CC01813K